ACCEPTOR AGGREGATION IN PM6:Y6 ORGANIC SOLAR CELL BLENDS REVEALED BY SPECTRAL DECOMPOSITION

Titas Klepeckas1, Dr. habil. Vidmantas Gulbinas1

1 Department of Molecular Compound Physics, Center for Physical Sciences and Technology, Lithuania

[email protected]

Recent advances in organic solar cells (OSCs) have been driven by the development of novel material systems, with PM6:Y6 blends emerging as promising candidates due to their power conversion efficiencies (PCEs) approaching 20%[1]. Although these efficiencies are impressive, certified OSC devices have recently surpassed this benchmark[2]. A major challenge limiting further performance improvements in PM6:Y6 systems is the incomplete understanding of the mechanisms underlying free charge carrier generation. One hypothesis suggests that free charge carriers are generated via energy cascades within the acceptor phase, where delocalized electrons migrate toward well-ordered aggregated domains, ultimately facilitating efficient charge separation[3]. This cascade mechanism may reduce recombination losses and enhance overall device performance.

In this study, we examine the role of acceptor aggregation in modulating exciton dissociation and charge separation in PM6:Y6 devices by employing spectral decomposition of the acceptor absorption spectra using Franck-Condon component analysis. Inspired by recent work from the Danie Khoh group[4], our method deconvolutes the complex absorption spectra of Y6 into distinct vibrational components, thereby distinguishing between aggregated and non-aggregated states. We observe that specific Franck–Condon vibrational progressions correlate with different molecular arrangements: well-ordered, aggregated Y6 domains exhibit red-shifted spectral features, whereas disordered regions display blue-shifted signatures.

By systematically varying the blend stoichiometry and thermal annealing conditions, we correlate the degree of Y6 aggregation with changes in the optical absorption profile and subsequent photocurrent generation. Our results indicate that a moderate degree of aggregation promotes exciton delocalization and enhances free charge carrier generation, thus facilitating more efficient charge separation at the donor-acceptor interface. In contrast, both excessive and insufficient aggregation lead to the formation of quasi-stable delocalized states or increased non-radiative recombination losses. Furthermore, time-resolved fluorescence measurements support the conclusion that aggregate formation modulates the local electronic environment, influencing the energy offset between excitonic and charge-transfer states.

Figure 1
Fig. 1. (a) Pristine acceptor absorption deconvolution. (b) Schematic of HOMO/LUMO levels in amorphous and aggregated phases, showing π-π interactions between acceptor cores (B) and end groups (G) with red arrows indicating electron energy cascades (adapted from Ref. [3]). (c) Relative intensities from the deconvoluted acceptor-rich blend absorption.


[1] Shoaee, S. et. al. What We Have Learnt from PM6:Y6. Adv. Mater. 2023, 35 (32), 2302005.

[2] Chen, Chen, et al. "Molecular interaction induced dual fibrils towards organic solar cells with certified efficiency over 20%." Nature Communications 15.1 (2024): 6865.

[3] Natsuda, Shin-ichiro, et al. "Cascaded energy landscape as a key driver for slow yet efficient charge separation with small energy offset in organic solar cells." Energy & Environmental Science 15.4 (2022): 1545-1555.

[4] Kroh, Daniel, et al. "Identifying the signatures of intermolecular interactions in blends of PM6 with Y6 and N4 using absorption spectroscopy." Advanced Functional Materials 32.44 (2022): 2205711.