MODELING OF ELECTROCHEMICAL-BASED IMMUNOSENSORS FOR THE DETECTION OF SPECIFIC ANTIBODIES

Maryia Drobysh1, Viktorija Liustrovaite2, Alma Rucinskiene3, Martynas Simanavicius4, Aurelija Zvirbliene4, Rimantas Slibinskas4, Ieva Plikusiene1, 2, Evaldas Ciplys4, Arunas Ramanavicius1, 2

1 Department of Functional Materials and Electronics, State Research Institute Center for Physical Sciences and Technology, Lithuania

2 Department of Physical Chemistry, Faculty of Chemistry and Geosciences, Vilnius University, Lithuania

3 Department of Electrochemical Materials Science, State Research Institute Center for Physical Sciences and Technology, Lithuania

4 Institute of Biotechnology, Life Sciences Center, Vilnius University, Lithuania

[email protected]

For the purpose to handle the ongoing pandemic of the coronavirus disease 2019 (COVID-19) rapid, specific, sensitive, and simple diagnosis methods are required. The causative agent of the COVID-19 is severe acute respiratory syndrome coronavirus 2 (SARS-CoV-2), whose RNA, structural proteins, or antibodies against it can act as target biomolecules for the detection of infection in a patient sample. Biosensors are widely used for the identifications of informational biomolecules, namely, nucleic acids [1] and proteins. The latter type includes immunosensors, which work principal is the detection of antigen-antibody coupling [2]. One of the most common types of immunosensors are based on electrochemistry, because of their affordability and simplicity without loss in accuracy and sensitivity.

Our study aimed to investigate the possibility to develop a novel method for viral disease diagnosis employing a common electrochemical technique. In our work, we used electrochemical impedance spectroscopy (EIS) as a powerful tool for observing the interaction between an immobilized virus antigen and antiviral antibodies at the modified working electrode surface. Immobilization of the antigen and formation of the antigen-antibody complex affected ion diffusion and electrical capacitance, thus influencing on electrochemical impedance of electrodes [3]. To immobilize the virus antigen on the working surface a self-assembled monolayer (SAM) was used, as an effective reusable tool for stable covalent binding of biomolecules to the different solid surfaces [4]. SAM modification was applied to the working gold electrode being part of an electrochemical cell that also included the platinum counter electrode and the reference [Ag/AgCl/KClsat] electrode.

Our experiments showed correspondences between impedimetric signals and stepwise modifications of electrode surface. We achieved a reproducible trend of significant increasing electrical impedance, i.e. electron-transfer resistance, on the key stage of antibody coupling. That fact indicates an increase in the layer thickness on the working surface and thereby testifies to the registered interaction. Hence, our outcome gives us the reason to suggest EIS-based immunosensor as an effective, rapid, easy to use, and to interpret detection tool. It is also worth noting that our experiment will serve as the basis for our further research in the field of electrochemical biosensors for the diagnosis of viral diseases in particular COVID-19.


[1] A. Ramanaviciene, A. Ramanavicius, Pulsed amperometric detection of DNA with an ssDNA/polypyrrole-modified electrode, Analytical and Bioanalytical Chemistry 379, 287-293 (2004).

[2] A. Ramanaviciene, N. German, et.al., Comparative study of surface plasmon resonance, electrochemical and electroassisted chemiluminescence methods based immunosensor for the determination of antibodies against human growth hormone, Biosensors Bioelectronics 36(1), 48-55 (2012).

[3] A. Ramanavicius, A. Finkelsteinas, et.al., Electrochemical impedance spectroscopy of polypyrrole based electrochemical immunosensor, Bioelectrochemistry 79(1), 11-16 (2010).

[4] A. Ramanaviciene, A. Kausaite-Minkstimiene, et.al., Comparative study of random and oriented antibody immobilization techniques on the binding capacity of immunosensor, Analytical Chemistry 82(15), 6401-6408 (2010).